HCID 67026976, compound → HCID 21804750, compound

Participants

Reaction Steps

A solution of 2-hydroxymethyl-6-methyl-isonicotinic acid methyl ester (500 mg, 2.76 mmol) in 32% aq. HCl (10 mL) is stirred at 60° C. for 5 h before it is evaporated and dried under HV to give the title compound as a yellow solid (480 mg); LC-MS: tR=0.16 min, [M+1]+=168.04.

Provenance & Evidence