HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 58418052, compound → HCID 58418008, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 58418052 | HCID 58418052 | — |
| Reactant | HCID 67026909 | HCID 67026909 | — |
| Product | HCID 58418008 | HCID 58418008 | — |
Reaction Steps
6-Ethyl-5-isobutyl-nicotinic acid is prepared in analogy to 5,6-diethyl-nicotinic acid from 5-chloro-6-vinyl-nicotinic acid tert.-butyl ester and 2,4,6-tri-(2-methyl-propenyl)-cycloboroxane pyridine complex (prepared in analogy to a procedure given by F. Kerins, D. F. O'Shea, J. Org. Chem. 67 (2002) 4968-4971); LC-MS: tR=0.64 min, [M+1]+=207.98.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08598208B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-de02c2d9859a4158a781da1526d5d927 |
| Source note | uspto-grants-2013_12 |