HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Isopropyl-6-methylisonicotinic acid ethyl ester → HCID 178426662, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Isopropyl-6-methylisonicotinic acid ethyl ester | HCID 66933504 | — |
| Reactant | HCID 178436634 | HCID 178436634 | — |
| Product | HCID 178426662 | HCID 178426662 | — |
Reaction Steps
The title compound is prepared in analogy to 2-ethyl-N-hydroxy-6-methyl-isonicotinamidine starting from 2-isopropyl-6-methyl-isonicotinic acid ethyl ester; LC-MS: tR=0.42 min, [M+1]+=194.08; 1H NMR (D6-DMSO): δ 1.22 (d, J=7.0 Hz, 6H), 2.44 (s, 3H), 2.91-3.02 (hept, J=7.0 Hz, 1H), 5.91 (s, 2H), 7.32 (s, 2H), 9.88 (s, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08598208B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-c260c0e5e4a748dab9b39eeec628bbc0 |
| Source note | uspto-grants-2013_12 |