HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Bromo-4-methoxy-2-pyridinecarboxylic acid → HCID 86657321, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Bromo-4-methoxy-2-pyridinecarboxylic acid | HCID 58418007 | — |
| Reactant | HCID 178426670 | HCID 178426670 | — |
| Product | HCID 86657321 | HCID 86657321 | 10.3% |
Reaction Steps
2-Bromo-6-[3-(2,6-dimethyl-4-pyridinyl)-[1,2,4]oxadiazol-5-yl]-4-methoxy-pyridine (24 mg) is prepared following the general method for the preparation of 3,5-dipyridyl-[1,2,4]oxadiazoles starting from 6-bromo-4-methoxy-pyridine-2-carboxylic acid (150 mg, 0646 mmol) and N-hydroxy-2,6-dimethyl-isonicotinamidine (107 mg, 0.646 mmol); LC-MS: tR=0.76 min, [M+1]+=360.91.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08598208B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-84b9dcd76b1e40bdabf2158a9721c5fc |
| Source note | uspto-grants-2013_12 |