HuagongsheHuagongshe Chemistry Print Report · For research reference only
Di-para-toluoyl-L-tartaric acid → HCID 131731065, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Di-para-toluoyl-L-tartaric acid | HCID 29414711 | — |
| Reactant | HCID 58058025 | HCID 58058025 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 131731065 | HCID 131731065 | 81.8% |
Reaction Steps
A solution that was prepared by dissolving 100.0 g of (R)-3-(t-butoxymethyl)piperazine-2-one to 500 mL of acetone, and then by dissolving 207.4 g of di-p-toluoyl-L-tartaric acid to 700 mL of acetone was slowly added to a reactor. The resulting reaction solution was stirred for 1 hour, and then resulting solid was filtered to obtain 251.4 g of a title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08598347B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-700d233806cd4e84a380f38859815a08 |
| Source note | uspto-grants-2013_12 |