HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-methyl-1H-imidazole-4-sulfonyl chloride → HCID 178481301, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-methyl-1H-imidazole-4-sulfonyl chloride | HCID 2736887 | — |
| Reactant | HCID 178479251 | HCID 178479251 | — |
| Product | HCID 178481301 | HCID 178481301 | — |
Reaction Steps
The title compound, white solid (19.5 mg, 45.3%), MS (ISP) m/z=475.1 [(M+H)+], was prepared in accordance with the general method of example 69 from Trans-4-[2-(4-Benzo[1,3]dioxol-4-yl-piperidin-1-yl)-ethyl]-cyclohexylamine (intermediate A) (30 mg, 90.8 mmol) and 1-methyl-1H-imidazole-4-sulfonyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08598357B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-5210cc6d4a574d6cb5ff0a14512b0f26 |
| Source note | uspto-grants-2013_12 |