HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron tribromide → 4-(4-Methylphenoxy)phenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron tribromide | HCID 25134 | — |
| Reactant | 1-Methoxy-4-(4-methylphenoxy)benzene | HCID 611840 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 4-(4-Methylphenoxy)phenol | HCID 641440 | — |
Reaction Steps
Following the general procedure for Example 12 (step 2), boron tribromide (1.0 M solution in dichloromethane, 7.75 mL, 7.75 mmol) was added to the product from step 1 (0.75 g, 3.50 mmol) in dichloromethane (10 mL) to afford the title compound was obtained (0.26 g, 36%) as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08598359B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-b69475b9633945b99bb8776fd5020009 |
| Source note | uspto-grants-2013_12 |