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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1909794Generated: October 31, 2026

Potassium Carbonate → HCID 59752954, compound

https://huagongshe.com/reaction/1909794

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
Reactant4-Methyloxybenzyl chlorideHCID 69993—
ReactantHCID 178420101HCID 178420101—
SolventMethyl Ethyl KetoneHCID 6569—
ProductHCID 59752954HCID 5975295489%

Reaction Steps

A mixture of 3-phenyl-1H-pyrazole (1.35 g, 9.36 mmol), 4-methoxybenzyl chloride (1.5 g, 9.7 mmol) and K2CO3 (3.3 g, 24.2 mmol) in methyl ethyl ketone was refluxed for 24 h. The salts were filtered off, and the solvent was removed in vacuo. The residue was purified by a column chromatography on silica gel to yield the title compound (2.2 g, 89%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08598359B2
Source datasetuspto-grants-2013_12
ORD IDord-69c940d0c7094c91951e5ee17b016b82
Source noteuspto-grants-2013_12