Triethylsilane → HCID 69000508, compound

HRID 1909806Notes

Reaction equation

HRID 1909806 reaction equation
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([CH:9]([C:11]2[O:12][C:13]([C:16]3[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=3)=[CH:14][CH:15]=2)O)=[CH:5][CH:4]=1.C([SiH](CC)CC)C>>[CH3:1][O:2][C:3]1[CH:4]=[CH:5][C:6]([CH2:9][C:11]2[O:12][C:13]([C:16]3[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=3)=[CH:14][CH:15]=2)=[CH:7][CH:8]=1

Participants

3

Reactant 2

HCID 12052TriethylsilaneHCID 68997754HCID 68997754, compound

Product 1

HCID 69000508HCID 69000508, compoundYield 99%

Procedure

The title compound (940 mg, 99%) was prepared from the product of step 2 (1.0 g, 3.6 mmol) and triethylsilane (2.3 g, 21.4 mmol) using the procedure of Example 159, step 3.

Sources & evidence

ORD record
ord-25454173c81446f3bb122578b660e773
Source dataset
uspto-grants-2013_12
Patent number
US08598359B2

Reaction notes

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