HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Methoxide → HCID 10536492, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | HCID 20098309 | HCID 20098309 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 10536492 | HCID 10536492 | 83.3% |
Reaction Steps
1.8 g (9.0 mmol) of 2-amino-6-fluoro-3-nitro-benzoic acid in methanol and 2.9 g (54 mmol) of NaOMe was heated at 90° C. overnight to produce 1.6 g (7.5 mmol 83%) of 2-amino-6-methoxy-3-nitro-benzoic acid. LCMS: 213 (M+1)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08598353B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-cb1d8a4dad2e46cc89521666e05c23df |
| Source note | uspto-grants-2013_12 |