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HRID1910253

反应详情

EQUATION

反应方程式

HRID 1910253 的结构方程式

REACTANTS

反应物

2
反应SMILES：[NH4+].[OH-]
HCID14923

Ammonium hydroxide

H5NO

反应SMILES：COc1c(F)c(F)c([N+](=O)[O-])c(C(=O)O)c1F
HCID21805474

2,4,5-Trifluoro-3-methoxy-6-nitrobenzoic acid

C8H4F3NO5

PRODUCTS

产物

1
反应SMILES：COc1c(F)c(N)c([N+](=O)[O-])c(C(=O)O)c1F
HCID86608397

未命名化合物

收率 80%

PROCEDURE

实验过程

2.0 g (8 mmol) of 3-methoxy-6-nitro-2,4,5-trifluoro-benzoic acid was treated with ammonium hydroxide to produce 1.6 g (6.45 mmol, 80%) of 3-amino-4,6-difluoro-5-methoxy-2-nitro-benzoic acid. LCMS: 249 (M+1)+.