O-Xylene → HCID 86676522, compound

HRID 1911712Notes

Reaction equation

HRID 1911712 reaction equation
[CH3:1][C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][C:7]=1[CH3:8].[C:9]1(=[O:15])[O:14][C:12](=[O:13])[CH:11]=[CH:10]1>>[CH3:1][C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][C:7]=1[CH3:8].[C:12]1(=[O:13])[O:14][C:9](=[O:15])[CH:10]=[CH:11]1

Participants

3

Reactant 2

HCID 7237O-XyleneHCID 7923Maleic Anhydride

Product 1

HCID 86676522HCID 86676522, compound

Procedure

To a 500 ml round bottom flask fitted with a mechanical stirrer, thermometer, air inlet bubbler and reflux condenser was added 65 g (0.61 moles) of o-xylene and 8.0 g (0.08 moles) of maleic anhydride. The solution was sparged with air then heated to reflux to initiate maleic anhydride free radical formation and then stirred for 6 hr. GC samples were taken at 2, 4 and 6 hr.

Workup

  1. customTo a 500 ml round bottom flask fitted with a mechanical stirrer
  2. temperaturethermometer, air inlet bubbler and reflux condenser
  3. customThe solution was sparged with air
  4. temperaturethen heated
  5. temperatureto reflux
  6. customwere taken at 2, 4 and 6 hr

Sources & evidence

ORD record
ord-0dd747d525f6464fb7b5bc5fb8f6cd9f
Source dataset
uspto-grants-2013_12
Patent number
US08604110B2

Reaction notes

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