HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 86230360, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | HCID 17604338 | HCID 17604338 | — |
| Catalyst | Zinc | HCID 23994 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 86230360 | HCID 86230360 | — |
Reaction Steps
{4-[(5-nitropyridin-2-yl)oxy]phenyl}methanol was subjected to reduction of nitro group by using zinc and acetic acid, the obtained compound reacted with methanesulfonyl chloride in pyridine, and the obtained compound was subjected to oxidation by using manganese dioxide to give the title compound having the following physical data.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08604207B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-3b133b62177949dc939609ae450cb453 |
| Source note | uspto-grants-2013_12 |