HRID1912102

反应详情

EQUATION

反应方程式

HRID 1912102 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

tert-Butyl (3-isobutylcyclobutyl)carbamate (2.90 g) and dioxane (15 mL) were mixed. To the mixture was added a solution of 4 N hydrochloric acid in dioxane (15 mL) at 10° C. The mixture was stirred at RT overnight. The reaction mixture was concentrated in vacuo to give the title compound (1.97 g) as a crude product.

WORKUP

后处理

  1. concentrationThe reaction mixture was concentrated in vacuo