HRID1912232

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：CSCC[C@H](NC(=O)OCC1c2ccccc2-c2ccccc21)C(=O)O

HCID2724632

N-[(9H-Fluoren-9-ylmethoxy)carbonyl]-L-methionine

C20H21NO4S

结构：CC(C)[C@H](N)C(=O)O.CC(N)N.CCC(=O)C1=CC(=O)NC1=O.NC(=O)C[C@H](N)C(=O)O

HCID131731084

未命名化合物

PRODUCTS

生成物

结构：CC(N)N.CCC(=O)C1=CC(=O)NC1=O.CSCC[C@H](N)C(=O)O.N[C@H](CC(=O)O)C(=O)O

HCID131731085

未命名化合物

PROCEDURE

实验过程

AF-Methionine-(D)Aspartic Acid-diaminoethane-propionyl maleimide (7d) was prepared using the same method as 5c starting with 100 mg of Fmoc-(D)Asp(OtBu)-diaminoethane-trityl resin (3), and using Fmoc-Met as AA1. Yield: 19.4 mg (25%) of white solid. RP-HPLC analysis: >95% at 10.97 min; ESMS m/z=1185.195 (M+H)+.