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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1912241Generated: November 2, 2026

Silica → N-(dipropylcarbamothioyl)-3,4,5-trimethoxybenzamide

https://huagongshe.com/reaction/1912241

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSilicaHCID 24261—
ReactantN-(dibutylcarbamothioyl)-3,4,5-trimethoxybenzamideHCID 12357718—
ProductN-(dipropylcarbamothioyl)-3,4,5-trimethoxybenzamideHCID 12357717—

Reaction Steps

A mixture of 90 parts by mass of PET obtained above and 10 parts by mass of silicon dioxide (“Silysia 445,” average particle size 2.5 μm, manufactured by Fuji Silysia Chemical Ltd.) was kneaded at 260° C. using a vented counter-rotation twin-axis extruder (L/D=35) with 30 mmφ, to prepare a PPT master (MS-4) containing 10% by mass of silicon dioxide.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08609227B2
Source datasetuspto-grants-2013_12
ORD IDord-349e197454b24492b94b51c9c718043d
Source noteuspto-grants-2013_12