4-Fluorophenylacetyl chloride → HCID 68751712, compound

Participants

Reaction Steps

The product from Example 105B and 4-fluorophenylacetyl chloride were processed using the method analogous to that described in Example 105C to afford the title compound. 1H NMR (300 MHz, DMSO-d6) δ ppm 1.38 (s, 9H), 3.63 (s, 2H), 6.99 (dd, J=7.1, 4.1 Hz, 1H), 7.13-7.18 (m, 2H), 7.31-7.41 (m, 2H), 8.48 (dd, J=4.1, 1.7 Hz, 1H), 8.91 (dd, J=7.1, 1.7 Hz, 1H), 9.94 (s, 1H); MS (DCI) m/z 327 (M+H)+.

Provenance & Evidence