HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(3,5-Difluorophenyl)acetyl chloride → HCID 68749155, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(3,5-Difluorophenyl)acetyl chloride | HCID 2782723 | — |
| Reactant | 3-Tert-butylpyrazolo[1,5-a]pyrimidin-2-amine | HCID 68755471 | — |
| Product | HCID 68749155 | HCID 68749155 | — |
Reaction Steps
The product from Example 105B and 3,5-difluorophenylacetyl chloride were processed using the method analogous to that described in Example 105C to afford the title compound. 1H NMR (300 MHz, DMSO-d6) δ ppm 1.39 (s, 9H), 3.70 (s, 2H), 6.98-7.16 (m, 4H), 8.49 (dd, J=4.1, 1.7 Hz, 1H), 8.92 (dd, J=6.8, 1.7 Hz, 1H), 10.01 (s, 1H); MS (DCI) m/z 345 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08609669B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-17444a69f2514dc499fc8917144007bd |
| Source note | uspto-grants-2013_12 |