HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexylacetyl chloride → HCID 68750173, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexylacetyl chloride | HCID 2757989 | — |
| Reactant | 3-Tert-butylpyrazolo[1,5-a]pyrimidin-2-amine | HCID 68755471 | — |
| Product | HCID 68750173 | HCID 68750173 | — |
Reaction Steps
The product from Example 105B and 2-cyclohexylacetyl chloride were processed using the method analogous to that described in Example 105C to afford the title compound. 1H NMR (300 MHz, DMSO-d6) δ ppm 0.92-1.03 (m, 2H), 1.11-1.29 (m, 3H), 1.44 (s, 9H), 1.59-1.81 (m, 6H), 2.18 (d, J=6.1 Hz, 2H), 6.99 (dd, J=7.1, 4.1 Hz, 1H), 8.47 (dd, J=4.1, 1.7 Hz, 1H), 8.92 (dd, J=7.1, 1.7 Hz, 1H), 9.64 (s, 1H); MS (DCI) m/z 315 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08609669B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-913c7119e8c94409a27ef1160ac9ade7 |
| Source note | uspto-grants-2013_12 |