Cyclopentylacetyl chloride → HCID 68756285, compound

Participants

Reaction Steps

The product from Example 105B and cyclopentylacetyl chloride were processed using the method analogous to that described in Example 105C to afford the title compound. 1H NMR (300 MHz, DMSO-d6) δ ppm 1.13-1.24 (m, 2H), 1.45-1.65 (m, 13H), 1.71-1.82 (m, 2H), 2.19-2.28 (m, 3H), 6.99 (dd, J=7.1, 4.1 Hz, 1H), 8.48 (dd, J=3.9, 1.9 Hz, 1H), 8.92 (dd, J=7.0, 1.9 Hz, 1H), 9.64 (br s, 1H); MS (DCI) m/z 301 (M+H)+.

Provenance & Evidence