HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methoxyphenylacetic Acid → HCID 68749192, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methoxyphenylacetic Acid | HCID 7690 | — |
| Reactant | 3-Tert-butylpyrazolo[1,5-a]pyrimidin-2-amine | HCID 68755471 | — |
| Product | HCID 68749192 | HCID 68749192 | — |
Reaction Steps
The product from Example 105B and 4-methoxyphenylacetic acid were processed using the method analogous to that described in Example 137 to afford the title compound. 1H NMR (300 MHz, DMSO-d6) δ ppm 1.39 (s, 9H), 3.55 (s, 2H), 3.74 (s, 3H), 6.87-6.97 (m, 2H), 6.99 (dd, J=7.1, 4.1 Hz, 1H), 7.23-7.26 (m, 2H), 8.47 (dd, J=3.9, 1.9 Hz, 1H), 8.91 (dd, J=7.0, 1.5 Hz, 1H), 9.87 (s, 1H); MS (DCI) m/z 339 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08609669B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-07b2a8195e14444b84a5e7ff7e721179 |
| Source note | uspto-grants-2013_12 |