3,4-Dichlorophenylacetic acid → HCID 68753250, compound

Participants

Reaction Steps

The product from Example 105B and 2-(3,4-dichlorophenyl)acetic acid were processed using the method analogous to that described in Example 137 to afford the title compound. 1H NMR (400 MHz, DMSO-d6/Deuterium Oxide) δ ppm 8.87 (d, J=5.9 Hz, 1H), 8.49 (dd, J=4.0, 1.8 Hz, 1H), 7.59-7.62 (m, 2H), 7.32-7.36 (m, 1H), 7.01 (dd, J=7.0, 4.0 Hz, 1H), 3.67-3.70 (bs, 2H), 1.39 (s, 9H); MS (ESI) m/z 377, 379 (M+H)+.

Provenance & Evidence