Hydrochloric Acid → HCID 68716544, compound

Participants

Reaction Steps

12 mg (0.03 mmol) of the compound from Example 23 are stirred in 1.5 ml of a 4 N solution of hydrogen chloride in dioxane for 30 min. The mixture is then decanted, the residue is stirred in tert-butyl methyl ether and decanted off again, and the solid that remains is initially air-dried and then dried under high vacuum.

Provenance & Evidence