Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Cesium carbonate | HCID 10796 | — |
| Reactant | HCID 66671930 | HCID 66671930 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 44125592 | HCID 44125592 | — |
Reaction Steps
21 mg (0.035 mmol) of the compound from Example 21A were initially charged in 0.69 ml of acetonitrile, and 45 mg (0.139 mmol) of cesium carbonate were added. The reaction mixture was stirred at 50° C. for 2 h and then cooled. The solid was filtered off and then washed with acetonitrile. The filtrate was concentrated and the residue was dried under high vacuum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08609686B2 |
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| Source dataset | uspto-grants-2013_12 |
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| ORD ID | ord-235f0e9498e94a2380db77deac065c7a |
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| Source note | uspto-grants-2013_12 |
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