反应详情

温度

50 °C

80 mg (0.15 mmol) of the compound from Example 47A were initially charged in 3 ml of acetonitrile, and 189 mg (0.58 mmol) of cesium carbonate were added. The mixture was stirred at 50° C. for 4 h. After cooling, the mixture was filtered and the filtrate was freed from the solvent on a rotary evaporator. The residue was dried under reduced pressure.

1. temperatureAfter cooling
2. filtrationthe mixture was filtered
3. customthe filtrate was freed from the solvent on a rotary evaporator
4. customThe residue was dried under reduced pressure