HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuryl chloride → HCID 19067199, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuryl chloride | HCID 24648 | — |
| Reactant | HCID 85885663 | HCID 85885663 | — |
| Product | HCID 19067199 | HCID 19067199 | — |
Reaction Steps
1-{[(Ethylthio)carbonyl]oxy}ethyl 2-methylpropionate (WO2005/66122) (412 mg) was cooled to −30° C. Sulfuryl chloride (157 μl) was added thereto, and the mixture was then stirred for 45 minutes. The solvent in the reaction solution was distilled off under reduced pressure to obtain a crude product of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08609710B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-4c9388d3f6914b59bd6bf7ca6ed00553 |
| Source note | uspto-grants-2013_12 |