HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aluminium lithium hydride → HCID 66663807, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Reactant | [(S)-6-(pyrrolidine-1-carbonyl)-1,2,3,4-tetrahydronaphthalen-2-yl]carbamic acid tert-butyl ester | HCID 66663930 | — |
| Product | HCID 66663807 | HCID 66663807 | — |
Reaction Steps
According to method B, [(S)-6-(pyrrolidine-1-carbonyl)-1,2,3,4-tetrahydro-naphthalen-2-yl]carbamic acid tert-butyl ester was reacted with lithium aluminum hydride (10 equiv., 60° C., 2 hours). The product was thus obtained with the molecular weight of 244.38 (C16H24N2); MS (ESI): 245 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08609731B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-db07546646794763b1e09e3b1776b9ac |
| Source note | uspto-grants-2013_12 |