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HRID1914104

反应详情

EQUATION

反应方程式

HRID 1914104 的结构方程式

REACTANTS

反应物

2
结构：O=C(O)c1ccncc1Cl
HCID2735816

3-chloroisonicotinic acid

C6H4ClNO2

结构：COc1ccc(C2=NN(C3CCNCC3)C(=O)C2(C)C)cc1OC.Cl
HCID66616406

未命名化合物

2 次

PRODUCTS

生成物

1
结构：COc1ccc(C2=NN(C3CCN(C(=O)c4ccncc4Cl)CC3)C(=O)C2(C)C)cc1OC
HCID46204651

未命名化合物

PROCEDURE

实验过程

The title compound is prepared analogously as described for GP2-WU2 using 5-(3,4-dimethoxyphenyl)-4,4-dimethyl-2-(piperidin-4-yl)-2,4-dihydro-3H-pyrazol-3-one (compound B1) and 3-chloroisonicotinic acid as starting compounds. The crude product is purified by chromatography (silica gel and DCM/diethyl ether/methanol=10:10:1) to yield the title compound.

WORKUP

后处理

  1. customThe title compound is prepared analogously
  2. customThe crude product is purified by chromatography (silica gel and DCM/diethyl ether/methanol=10:10:1)