4-Vinylbenzoic acid → HCID 86649830, compound
Reaction equation
[CH:1]([C:3]1[CH:11]=[CH:10][C:6]([C:7]([OH:9])=[O:8])=[CH:5][CH:4]=1)=[CH2:2].[Ag:12]=O>C(#N)C>[CH:1]([C:3]1[CH:11]=[CH:10][C:6]([C:7]([O-:9])=[O:8])=[CH:5][CH:4]=1)=[CH2:2].[Ag+:12]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Conditions
- Temperature
- 23 °C
Procedure
A mixture of 3.08 parts of 4-vinylbenzoic acid and 15.00 parts of acetonitrile was stirred at 23° C. for 30 minutes. To the resultant mixture, 2.32 parts of silver oxide was added. The obtained mixture was stirred at 23° C. for 4 hours, and then, filtrated. The obtained solid was mixed with 10 parts of tert-butyl methyl ether and the resultant mixture was stirred at 23° C. for 30 minutes. The mixture was filtrated and the obtained solid was dried to obtain 4.34 parts of silver 4-vinylbenzoate.
Workup
- stirringThe obtained mixture was stirred at 23° C. for 4 hours
- filtrationfiltrated
- additionThe obtained solid was mixed with 10 parts of tert-butyl methyl ether
- stirringthe resultant mixture was stirred at 23° C. for 30 minutes
- filtrationThe mixture was filtrated
- customthe obtained solid was dried
Sources & evidence
- ORD record
- ord-200cbaf639bd48cba6e6d7909291a16b
- Source dataset
- uspto-grants-2013_12
- Patent number
- US08614046B2
Reaction notes
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