HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Aminobenzyl alcohol → HCID 49780152, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Aminobenzyl alcohol | HCID 21439 | — |
| Reactant | 3-Bromobenzaldehyde | HCID 76583 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 49780152 | HCID 49780152 | 6.5% |
Reaction Steps
A mixture of 2-amino-benzenemethanol (0.073 mol) and 3-bromo-benzaldehyde (0.073 mol) in 2-propanol (100 mL) was stirred for 3 hours at rt. The solvent was evaporated. Part (3 g) of the residue (20.5 g) was crystallized from hexane. The precipitate was filtered off and dried, yielding 1.37 g of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08614201B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-4d316b75241541c79723d0a256e5f9a2 |
| Source note | uspto-grants-2013_12 |