N-Iodosuccinimide → HCID 178433771, compound

Participants

Reaction Steps

To a solution of Compound (1-3) (0.2 g, 0.73 mmol, 1 eq.) in DMF (10 mL) was added N-iodosuccinimide (0.18 g, 0.8 mmol, 1.1 eq.) and the mixture stirred for 2 hours and concentrated. The residue was purified by silica gel chromatography using CHCl3/MeOH (10%) as eluant to give Compound (17-1)

Provenance & Evidence