HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus oxychloride → HCID 58034613, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | HCID 136133173 | HCID 136133173 | — |
| Product | HCID 58034613 | HCID 58034613 | — |
Reaction Steps
In a 20 mL scintillation vial Compound (19-1) (0.08 g, 0.275 mmol, 1.0 eq.) was heated with 2 mL of POCl3 at 80° C. for 2 hours. The reaction was cooled and concentrated and the residue by silica gel chromatography using CHCl3/MeOH (10%) as eluant to give Compound (19-2).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08614221B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-d7c827809a954340965a77a589b884ad |
| Source note | uspto-grants-2013_12 |