HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 52945927, compound → HCID 54768028, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 52945927 | HCID 52945927 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 54768028 | HCID 54768028 | — |
Reaction Steps
20 mL of methanol was slowly added dropwise to the compound (b) prepared in Preparation 2 (1.31 mmol, 1 eq) and 5% Pd/C (0.4 g), and then the reaction mixture was charged with hydrogen and stirred at room temperature for 24 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08614240B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-c2b17ff91e9847e6823d035bf45e0eca |
| Source note | uspto-grants-2013_12 |