HuagongsheHuagongshe Chemistry Print Report · For research reference only
Titanium tetrabutoxide → HCID 131731098, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Titanium tetrabutoxide | HCID 21801 | — |
| Reactant | HCID 46901656 | HCID 46901656 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 131731098 | HCID 131731098 | 98.8% |
Reaction Steps
166 g (1 mol) of ethyl(2-methyl-3-hydroxypropyl)phosphinic acid (produced as in Example 5) and 85 g of titanium tetrabutoxide are refluxed in 500 ml of toluene for 40 hours. The resulting butanol is distilled off from time to time with proportions of toluene. The solution formed is subsequently freed of solvent to leave 161 g (91% of theory) of ethyl(3-hydroxypropyl)phosphinic acid titanium salt.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08614267B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-c1a50d46b5324158944b2c153da31777 |
| Source note | uspto-grants-2013_12 |