HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1914985Generated: October 30, 2026
6-Bromohexanoic acid → HCID 178433620, compound
https://huagongshe.com/reaction/1914985
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 6-Bromohexanoic acid | HCID 20210 | — |
| Reactant | 2,3,3-Trimethyl-3H-pyrrolo[2,3-b]pyridine | HCID 22266836 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 178433620 | HCID 178433620 | — |
Reaction Steps
A mixture of 0.54 g of 2,3,3-trimethyl-3H-pyrrolo[2,3-b]pyridine and 1.32 g of 6-bromohexanoic acid is heated at 120° C. for one hour. Ethyl acetate (10 mL) is added, and the reaction mixture is heated at reflux for 15 minutes, then cooled to room temperature. The supernatant liquid is decanted to yield the product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08614302B2 |
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| Source dataset | uspto-grants-2013_12 |
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| ORD ID | ord-930f2b60b49a47ae8d4deaa77b1eaaca |
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| Source note | uspto-grants-2013_12 |
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