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HRID1914994

反应详情

EQUATION

反应方程式

HRID 1914994 的结构方程式

REACTANTS

反应物

3
结构：ClP(Cl)(Cl)(Cl)Cl
HCID24819

Phosphorus pentachloride

Cl5P

结构：CCN1c2ccccc2C(CS(=O)(=O)Cl)=CC1(C)C
HCID12138182

未命名化合物

结构：CCN1c2cc(OC)ccc2C(CS(=O)(=O)O)=CC1(C)C
HCID12138189

未命名化合物

PRODUCTS

生成物

1
结构：CCN1c2cc(OC)ccc2C(CS(=O)(=O)Cl)=CC1(C)C
HCID12138190

未命名化合物

收率 73%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：c1ccccc1
溶剂HCID241

Benzene

C6H6

PROCEDURE

实验过程

(1-Ethyl-7-methoxy-2,2-dimethyl-1,2-dihydroquinol-4-yl)-methanesulfonic acid chloride (16) is prepared similarly to compound (9) from compound (15) and phosphorus pentachloride in dry benzene. The acid chloride that is obtained is immediately used for further reaction.