HuagongsheHuagongshe Chemistry Print Report · For research reference only
Guanidine Hydrochloride → HCID 68463935, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Guanidine Hydrochloride | HCID 5742 | — |
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | HCID 67027749 | HCID 67027749 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 68463935 | HCID 68463935 | — |
Reaction Steps
5 g of the product of step 1 and 3 g guanidine hydrochloride are dissolved in 100 ml methanol and 2.7 g of NaOMe is added. The mixture is heated to reflux for 17 h. The product is precipitated upon dilution of the mixture with water and is collected by filtration and washed twice with water.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08614218B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-06bdbd254c7e430e9defd9888fb2fd55 |
| Source note | uspto-grants-2013_12 |