Hydrogen Bromide → 2-[(4-Bromophenyl)amino]benzothiazol-5-ol

HRID 1915620Notes

Reaction equation

HRID 1915620 reaction equation
[Br:1][C:2]1[CH:7]=[CH:6][C:5]([NH:8][C:9]2[S:10][C:11]3[CH:17]=[CH:16][C:15]([O:18]C)=[CH:14][C:12]=3[N:13]=2)=[CH:4][CH:3]=1.Br>>[Br:1][C:2]1[CH:3]=[CH:4][C:5]([NH:8][C:9]2[S:10][C:11]3[CH:17]=[CH:16][C:15]([OH:18])=[CH:14][C:12]=3[N:13]=2)=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 260Hydrogen BromideHCID 7489958N-(4-bromophenyl)-5-methoxy-1,3-benzothiazol-2-amine

Product 1

HCID 220408762-[(4-Bromophenyl)amino]benzothiazol-5-ol

Procedure

The mixture of (4-bromophenyl)(5-methoxybenzothiazol-2-yl)amine and hydrobromic acid (48%) was subjected to the microwave at 150° C. for 6 mins to yield the desired product. MS: MH+=321

Sources & evidence

ORD record
ord-d011b15ead434fd79d9d3512ce26a930
Source dataset
uspto-grants-2013_12
Patent number
US08614330B2

Reaction notes

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