4-Iodoaniline → HCID 67364245, compound

HRID 1916601Notes

Reaction equation

HRID 1916601 reaction equation
I[C:2]1[CH:8]=[CH:7][C:5]([NH2:6])=[CH:4][CH:3]=1.[Cl:9][C:10]1[CH:15]=[CH:14][C:13]([C:16]2[CH:17]=[CH:18][C:19]([C:22]#[CH:23])=[N:20][CH:21]=2)=[CH:12][CH:11]=1>>[Cl:9][C:10]1[CH:11]=[CH:12][C:13]([C:16]2[CH:17]=[CH:18][C:19]([C:22]#[C:23][C:2]3[CH:8]=[CH:7][C:5]([NH2:6])=[CH:4][CH:3]=3)=[N:20][CH:21]=2)=[CH:14][CH:15]=1

Participants

3

Reactant 2

HCID 108934-IodoanilineHCID 578453285-(4-Chloro-phenyl)-2-ethynyl-pyridine

Product 1

HCID 67364245HCID 67364245, compound

Procedure

Prepared according to general working method I from 4-iodoaniline (732 mg, 3.28 mmol) and 5-(4-chloro-phenyl)-2-ethynyl-pyridine (700 mg, 3.28 mmol).

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-e521f938f7764d7483b3d8584730c4c8
Source dataset
uspto-grants-2013_12
Patent number
US08618132B2

Reaction notes

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