HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 67363753, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 62640828 | HCID 62640828 | — |
| Solvent | Formic Acid | HCID 284 | — |
| Product | HCID 67363753 | HCID 67363753 | — |
Reaction Steps
A solution of 470 mg (1.65 mmol) 5-bromo-N2-(2-pyrrolidin-1-yl-ethyl)-pyridine-2,3-diamine in 10 mL formic acid is refluxed for 1.5 h. The mixture is made alkaline with saturated K2CO3 solution and extracted with 40 mL EtOAc. The organic phase is dried over Na2SO4 and the solvent is eliminated i.vac.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08618132B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-145ecbdc1fb34f3ba9e782d0da06c36a |
| Source note | uspto-grants-2013_12 |