HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyrrolidine → HCID 2824673, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyrrolidine | HCID 31268 | — |
| Reactant | 2-chloro-N-(4-iodophenyl)acetamide | HCID 735792 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 2824673 | HCID 2824673 | — |
Reaction Steps
1.53 mL (18.6 mmol) pyrrolidine are added to a solution of 2.20 g (7.45 mmol) 2-chloro-N-(4-iodo-phenyl)-acetamide in 50 mL DCM. The reaction solution is stirred overnight at RT. The mixture is filtered, the filtrate dried over MgSO4 and the solvent is eliminated i.vac.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08618132B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-9eece8b3b1a648989db2fec8935feae1 |
| Source note | uspto-grants-2013_12 |