HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 10635707, compound → 6-Bromoquinolin-2(1H)-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 10635707 | HCID 10635707 | — |
| Solvent | Sulfuric Acid | HCID 1118 | — |
| Product | 6-Bromoquinolin-2(1H)-one | HCID 12378943 | — |
Reaction Steps
37.8 g (0.14 mol) (E)-N-(4-bromo-phenyl)-3-ethoxy-acrylamide are added batchwise to 200 mL concentrated sulphuric acid and stirred for 2 h at RT. Then the reaction mixture is poured into ice water, the precipitate is filtered off and washed with water. The solid is dried at 70° C. in the drying cupboard.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08618132B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-053f5ee3423049e3b6ff14ee814fdd79 |
| Source note | uspto-grants-2013_12 |