HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 59835762, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | HCID 59835738 | HCID 59835738 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 59835762 | HCID 59835762 | — |
Reaction Steps
16 μL (170 μmol) acetic anhydride are added to a solution of 35 mg (84 μmol) 5-[5-(4-chloro-phenyl)-pyridin-2-ylethynyl]-2-(2-pyrrolidin-1-yl-ethoxy)-phenylamine in 2 mL DCM and the reaction mixture is stirred overnight at RT and then purified by chromatography on silica gel (gradient: EtOAc to EtOAc/MeOH/NH3 7:3:0.3) without any further working up
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08618132B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-c50f6e32596444bb88406bf9cd2aface |
| Source note | uspto-grants-2013_12 |