HCID 67954034, compound → HCID 67953928, compound

Participants

Reaction Steps

Compound 15-C (0.820 g, 1.71 mmol) was dissolved in 4N HCl in dioxane (44 mL) and the reaction mixture was stirred for 24 h at room temperature. The solvent was evaporated in vacuo and the crude product was washed with ethyl ether. The resulting solid was filtered, washed with additional ethyl ether, and dried in vacuo to give compound 15-D as a white solid (0.610 g, 86%); MS m/z (M+H+) 380.

Provenance & Evidence