4-Iodoaniline → HCID 56589685, compound

HRID 1916998Notes

Reaction equation

HRID 1916998 reaction equation
[C:1]12([CH:7]3[CH2:8][CH2:9][CH:4]1[CH:5]1[C:13](=[O:14])[O:12][C:10](=[O:11])[CH:6]13)[CH2:3][CH2:2]2.[I:15][C:16]1[CH:22]=[CH:21][C:19]([NH2:20])=[CH:18][CH:17]=1>C(Cl)(Cl)Cl>[I:15][C:16]1[CH:22]=[CH:21][C:19]([NH:20][C:10]([C@@H:6]2[C@H:7]3[C:1]4([CH2:3][CH2:2]4)[C@H:4]([CH2:9][CH2:8]3)[C@@H:5]2[C:13]([OH:12])=[O:14])=[O:11])=[CH:18][CH:17]=1

Participants

4

Reactant 2

HCID 108934-IodoanilineHCID 585803091418115-02-2

Product 1

HCID 56589685HCID 56589685, compound

Reagents, catalysts & solvents 1

HCID 6212ChloroformSolvent

Procedure

Following General Procedure A, Compound 2 (0.084 g, 0.44 mmol) and 4-iodoaniline (0.090 g, 0.44 mmol) in chloroform (6 mL) were converted into the title compound, which was isolated as a white solid.

Sources & evidence

ORD record
ord-c70f140a816f43f1a1d3739d3d5c10d9
Source dataset
uspto-grants-2013_12
Patent number
US08618163B2

Reaction notes

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