Phenol, o-mercapto-(6CI,7CI,8CI) → HCID 66593635, compound

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Reaction Steps

This compound was prepared in 58% yield from 2-mercaptophenol and neopentyl iodide according to the procedure for 1p in Example VIII. 1H NMR (CDCl3): δ 1.03 (s, 9H), 2.70 (s, 2H), 6.72 (s, 1H), 6.83-6.87 (m, 1H), 6.96 (dd, J=2.2 Hz, J=7.95, 1H), 7.21-7.26 (m, 1H), 7.46-7.48 (m, 1H); 13C NMR (CDCl3): δ 28.90, 32.56, 52.64, 114.82, 120.94, 130.74, 135.61, 156.60, 158.89;

Provenance & Evidence