HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid Mixture with Hydrobromic Acid → Hydrogen Bromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid Mixture with Hydrobromic Acid | HCID 21893785 | — |
| Reactant | HCID 57864657 | HCID 57864657 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | Hydrogen Bromide | HCID 260 | — |
| Product | HCID 68637628 | HCID 68637628 | — |
Reaction Steps
The starting material 30 (200 mg) was treated with 3 mL of HBr/AcOH solution for 1 h. To the reaction mixture was added diethyl ether (20 mL). The white solid was filtered to give the title compound as HBr salt. Yield: 182 mg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08618282B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-8c15644a12924d57831855c45c029709 |
| Source note | uspto-grants-2013_12 |