HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-bromo-4-methyl-1,2,4-triazine-3,5(2h,4h)-dione → Toluene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-bromo-4-methyl-1,2,4-triazine-3,5(2h,4h)-dione | HCID 260564 | — |
| Reactant | 1-(2-Trifluoromethylbenzoyl)piperazine hydrochloride | HCID 16733783 | — |
| Product | Toluene | HCID 1140 | 27% |
| Product | 4-methyl-6-[4-(2-trifluoromethyl-benzoyl)-piperazin-1-yl]-2H-[1,2,4]triazine-3,5-dione | HCID 44621496 | — |
Reaction Steps
The compound 4 (solid) is prepared from the triazine 2a and the intermediate 6a according to the synthesis method 1 in toluene (yield: 27%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08618287B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-93af7624adb948a9833888fe21881cf8 |
| Source note | uspto-grants-2013_12 |