HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Bromo-2,4-dimethyl-2,3,4,5-tetrahydro-1,2,4-triazine-3,5-dione → Toluene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Bromo-2,4-dimethyl-2,3,4,5-tetrahydro-1,2,4-triazine-3,5-dione | HCID 260563 | — |
| Reactant | 1-(2-Trifluoromethylbenzoyl)piperazine hydrochloride | HCID 16733783 | — |
| Product | Toluene | HCID 1140 | 55% |
| Product | 2,4-dimethyl-6-[4-(2-trifluoromethyl-benzoyl)-piperazin-1-yl]-2H-[1,2,4]triazine-3,5-dione | HCID 44621497 | — |
Reaction Steps
The compound 5 (solid) is prepared from the triazine 1b and the intermediate 6a according to the synthesis method 1 in toluene (yield: 55%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08618287B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-5d595c5838814334aba6ea04c9e257df |
| Source note | uspto-grants-2013_12 |