HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Bromo-2,4-dimethyl-2,3,4,5-tetrahydro-1,2,4-triazine-3,5-dione → 1-Butanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Bromo-2,4-dimethyl-2,3,4,5-tetrahydro-1,2,4-triazine-3,5-dione | HCID 260563 | — |
| Reactant | 4-(2-Chlorophenoxy)piperidine | HCID 3864656 | — |
| Product | 1-Butanol | HCID 263 | 60% |
| Product | HCID 44621507 | HCID 44621507 | — |
Reaction Steps
The compound 27 (solid) is prepared from the triazine 1b and from the intermediate 8a according to the synthesis method 1 in n-butanol (yield: 60%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08618287B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-f381bceee48b4c6592cb6155e1d75349 |
| Source note | uspto-grants-2013_12 |